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Beilstein J. Org. Chem. 2009, 5, No. 26, doi:10.3762/bjoc.5.26
Graphical Abstract
Scheme 1: Flavin–guanidinium ion conjugates 1 and 2 and tetraacetyl riboflavin (3).
Scheme 2: Synthesis of flavins 1 and 2. Conditions: (i) DMAP, H2O, Δ, 20 h, 71–78%, (ii) HOBt, EDC, NEt(iPr)2...
Figure 1: X-ray crystal structures of the flavin-Kemp’s acids 6 (left) and 9 (right).
Figure 2: Structure of compound 1 in the solid state.
Figure 3: Calculated lowest energy conformation of 1 in the gas phase (AM1, Spartan program package).
Scheme 3: Oxidative photocleavage of dibenzyl phosphate.
Scheme 4: Photoreduction of 4-nitrophenyl phosphate.
Scheme 5: Photo Diels–Alder-reaction of anthracene with N-methyl-maleinimide.